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A novel synthesis of α-(phenylthio)aldehydes

✍ Scribed by B. J. M. Jansen; R. M. Peperzak; Ae. de Groot

Book ID
104588837
Publisher
Elsevier Science
Year
2010
Tongue
English
Weight
561 KB
Volume
106
Category
Article
ISSN
0165-0513

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α-Sulfenylation of acylsilanes and aldeh
α-Sulfenylation of acylsilanes and aldehydes with N-(phenylthio)succinimide
✍ Chih-Hao Huang; Kang-Shyang Liao; Surya Kanta De; Yeun-Min Tsai 📂 Article 📅 2000 🏛 Elsevier Science 🌐 French ⚖ 135 KB

The reactions of acylsilanes with N-(phenylthio)succinimide in the presence of p-toluenesulfonic acid in acetonitrile give α-sulfenylated acylsilanes in good yields. Aldehydes with α-alkyl substituent afford moderate yields of α-sulfenylated products under the same conditions.