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A Novel Layered Mixed-Valence Vanadium Phenanthroline Complex: Hydrothermal Synthesis and Crystal Structure of [VIVVV2O7(phen)]n

✍ Scribed by Duan, Chung-ying; Tian, Yu-peng; Lu, Zhong-lin; You, Xiao-zeng; Huang, Xiao-ying

Book ID: 126481577
Publisher: American Chemical Society
Year: 1995
Tongue: English
Weight: 158 KB
Volume: 34
Category: Article
ISSN: 0020-1669
DOI: 10.1021/ic00105a001

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Blue crystals of Cu 2 (phen) 2 (H 2 O) 2 (C 5 H 6 O 4 ) 2 were obtained from a CH 3 OH±H 2 O solution containing CuCl 2 , 1,10-phenanthroline (phen), glutaric acid and Na 2 CO 3 . The crystal structure (monoclinic, P2 1 /c (no. 14), a = 10.271(1), b = 10.595(1), c = 15.585(1) A Ê , b = 107.105(3)°,