✦ LIBER ✦

A non-exchange synthesis of tritium-labelled tetrahydrocannabinols

✍ Scribed by E. W. Gill; Gareth Jones

Publisher: John Wiley and Sons
Year: 1972
Tongue: French
Weight: 394 KB
Volume: 8
Category: Article
ISSN: 0022-2135
DOI: 10.1002/jlcr.2590080209

No coin nor oath required. For personal study only.

✦ Synopsis

A NON-EXCHANGE SYNTHESIS OF TRITIUM-LABELLED TETRAHYDROCANNABINOLS I E. W. G i l l a n d G a r e t h Jones. U n i v e r s i t y D e p a r t m e n t o f P h a r m a c o l o g y , S o u t h P a r k s R o a d , O x f o r d , E n g l a n d . R e c e i v e d o n O c t o b e r 5 , 1 9 7 1 .

SUMMARY T r i t i u m -l a b e l l e d ( -) -A 1 ( 6 * a n d I-)-A'-tetrahy?rocann a b i n o l s a t a s p e c i f i c a c t i v i t y o f 607 mCi/mmole were s y n t h e s i a e d by a non-exchange method. The t r it i u m was i n t r o d u c e d by t h e c a t a l y t i c r e d u c t i o n w i t h t r i t i u m gas

of an u n s a t u r a t e d p r e c u r s o r o f d i m e t h y l o l i v e t o l i n h e x a f l u o r o b e n z e n e a s a non-exchanging s o l v e n t . S p e c i f i c a l l y l a b e l l e d o t i v e t o l was subse-

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