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Synthesis of tritium labelled catechol

✍ Scribed by K. K. Hwang; B. Bhooshan; R. E. Kouri; C. J. Henry

Publisher: John Wiley and Sons
Year: 1982
Tongue: French
Weight: 154 KB
Volume: 19
Category: Article
ISSN: 0022-2135
DOI: 10.1002/jlcr.2580190106

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✦ Synopsis

Abstract

The preparation of tritium labelled catechol by catalytic reduction of tetrabromocatechol is described. Recrystallization of catechol (U‐^3^H) after silica gel column purification gave 68% yield of the desired product with 98% purity as assayed by high performance liquid chromatography.

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