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A new type of multilayer system–silver(I) complexes of polycyclic aromatic compounds

✍ Scribed by Megumu Munakata; Liang Ping Wu; Gui Ling Ning

Publisher
Elsevier Science
Year
2000
Tongue
English
Weight
785 KB
Volume
198
Category
Article
ISSN
0010-8545

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✦ Synopsis

A new type of silver(I) coordination complex derived from silver(I) perchlorate (or triflate) and polycyclic aromatic compounds is reviewed. Structural studies by single-crystal X-ray diffraction have shown that all compounds contain extended one-to three-dimensional structures in which several metal atoms are sandwiched between two fused polycyclic systems. Special attention is paid to the combination of the plasticity of the metal ion,

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The reaction of 4-amino-6-methyl-1,2,4-triazine-3(2 H)-thione-5-one (AMTTO) with silver(I) nitrate in methanol gives the complex [Ag(AMTTO) 2 ]NO 3 (1). 1 was characterized by IR and 13 C NMR spectroscopy and by an X-ray structure analysis [space group C2/c, Z = 4, lattice dimensions at ±80 °C: a =