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A new route to ?-fluoromethyl- and ?-fluoroalkyl-phosphonates

✍ Scribed by Patois, Carl; Savignac, Philippe

Book ID
120015524
Publisher
The Royal Society of Chemistry
Year
1993
Tongue
English
Weight
203 KB
Volume
22
Category
Article
ISSN
0022-4936

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Starting from diethyl benzylphosphonates, a wide variety of diethyl ot-monofluoro, chloro, bromo and iodobenzylphosphonates have been obtained in pure form by a one-pot procedure. This high yielding method implies the intermediate protection of the benzyl anion with TMSC1 followed by halogenation wi