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A New, High-Yield Synthesis of Tetraphosphacubanes

✍ Scribed by Dr. Thomas Wettling; Dipl.-Chem. Bernhard Geissler; Dr. Ronald Schneider; Dipl.-Chem. Stefan Barth; Prof. Dr. Paul Binger; Prof. Dr. Manfred Regitz


Publisher
John Wiley and Sons
Year
1992
Tongue
English
Weight
257 KB
Volume
31
Category
Article
ISSN
0044-8249

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A high yield synthesis of 2-14C-methimaz
✍ Philip W. Lee; Michael J. Gudzinowicz; Robert A. Neal πŸ“‚ Article πŸ“… 1978 πŸ› John Wiley and Sons 🌐 French βš– 156 KB

C-Methimazole was prepared in a condensation reaction between meth laminoacetaldehyde dimethyl acetal and potassium ''C-thiocyanate in acidic medium. The yield of final product was 86.3% of theoretical with a radio purity of greater than 99.5%.