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A high yield synthesis of 2-14C-methimazole

✍ Scribed by Philip W. Lee; Michael J. Gudzinowicz; Robert A. Neal

Publisher
John Wiley and Sons
Year
1978
Tongue
French
Weight
156 KB
Volume
14
Category
Article
ISSN
0022-2135

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✦ Synopsis

C-Methimazole was prepared in a condensation reaction between meth laminoacetaldehyde dimethyl acetal and potassium ''C-thiocyanate in acidic medium. The yield of final product was 86.3% of theoretical with a radio purity of greater than 99.5%.

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