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A new 1D metal–organic coordination polymer with blue fluorescent emission: [Cd2(1,10′-phen)2(betc)(H2O)]n

✍ Scribed by Xiaojun Gu; Yanhui Chen; Jun Peng; Zhenyu Shi; Enbo Wang; Ninghai Hu

Publisher
Elsevier Science
Year
2004
Tongue
English
Weight
199 KB
Volume
697
Category
Article
ISSN
0022-2860

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## Abstract A novel 3D polymeric Pb^II^ complex involving three different hemidirected Pb^II^ coordination spheres, [Pb~3~(phen)~3~(H~2~O)~2~(sip)~2~]~__n__~⋅3 H~2~O (phen=1,10‐phenanthroline and sip=5‐sulfoisophthalate=5‐sulfobenzene‐1,3‐dicarboxylate), was synthesized and characterized by element

Crystal Structures of 3.0.CO;2-Z/asset/e
Crystal Structures of 3.0.CO;2-Z/asset/equation/tex2gif-stack-1.gif?v=1&t=h5l6migq&s=c6023d23614cc5febe987fafc1b321310df66e88" class="inlineGraphic">{[Cd(phen)](C6H8O4)3/3} and 3.0.CO;2-Z/asset/equation/tex2gif-stack-2.gif?v=1&t=h5l6migr&s=ca7048152611c2fb5494587a82e9d48966405110" class="inlineGraphic">{[Cd(phen)](C7H10O4)3/3} · 2H2O with C6H10O4 = Adipic Acid and C7H12O4 = Pimelic Acid
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Two coordination polymers 1 ϱ {[Cd(phen)](C 6 H 8 O 4 ) 3/3 } (1) and 1 ϱ {[Cd(phen)](C 7 H 10 O 4 ) 3/3 } • 2H 2 O (2) were structurally characterized by single crystal X-ray diffraction methods. In 1 (C2/ c (no. 15), a ϭ 16.169(2) A ˚, b ϭ 15.485(2) A ˚, c ϭ 14.044(2) A ˚, β ϭ 112.701(8)°, U ϭ 324