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A mild oxidative method for the preparation of γ-hydroxy-α-nitroolefins from α,β-epoxyketoximes using IBX

✍ Scribed by Alba Souto; Jaime Rodríguez; Carlos Jiménez

Publisher
Elsevier Science
Year
2009
Tongue
French
Weight
234 KB
Volume
50
Category
Article
ISSN
0040-4039

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A wide variety of alpha-diazo-beta-ketoesters can be prepared in good overall yields via a two-step sequence involving addition of ethyl lithiodiazoacetate to aliphatic, aromatic and conjugated aldehydes followed by mild oxidation with the Dess-Martin periodinane.