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A Low Pressure Method for Wolff—Kishner Reduction

✍ Scribed by Soffer, Milton D.; Soffer, Mary Barns; Sherk, Kenneth W.

Book ID
127057678
Publisher
American Chemical Society
Year
1945
Tongue
English
Weight
244 KB
Volume
67
Category
Article
ISSN
0002-7863

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Two homoallyl/cyclopropylalkyl rearrange
Two homoallyl/cyclopropylalkyl rearrangements accompanying a Wolff–Kishner type reduction
✍ Manfred Schlosser; Armin Zellner 📂 Article 📅 2001 🏛 Elsevier Science 🌐 French ⚖ 77 KB

Conceived as a model study for the enantioselective synthesis of the natural product (S)-bakuchiol, the deoxygenation of a recently described trishomoallyl alcohol was attempted using the Kabalka modification of the Wolff-Kishner method after prior oxidation of the alcohol to the ketone. However, an