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A Practical, Kilogram-Scale Implementation of the Wolff−Kishner Reduction

✍ Scribed by Kuethe, Jeffrey T.; Childers, Karla G.; Peng, Zhihui; Journet, Michel; Humphrey, Guy R.; Vickery, Thomas; Bachert, Donald; Lam, Thientu T.

Book ID
111643337
Publisher
American Chemical Society
Year
2009
Tongue
English
Weight
220 KB
Volume
13
Category
Article
ISSN
1083-6160

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The cleavage of two carbon-carbon bonds
The cleavage of two carbon-carbon bonds in a Wolff-Kishner reduction
✍ Robert P. Lemieux; Peter Beak 📂 Article 📅 1989 🏛 Elsevier Science 🌐 French ⚖ 188 KB

The reaction of dispiro[cyclopropane-l,l'-indan-3',1"-cyclopropane]-2'-one (1) under Wolff-Kishner conditions gives spiro[cyclopropane-l,l'-indan] (2) in which the ketone has been reduced and two bonds of one cyclopropane ring have been cleaved. The Wolff-Kishner reaction is a classic method for