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A limitation to the preparation of β,α -unsaturated n,n-dialkyl amides starting from β,α -unsaturated acid chlorides

✍ Scribed by Renzo Rossi; Giovanni Ingrosso


Publisher
Elsevier Science
Year
1969
Tongue
French
Weight
130 KB
Volume
10
Category
Article
ISSN
0040-4039

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β-Alkyl and β-Alkyl-α-Hydroxy Carboxylic
✍ Dipl.-Chem. Karola Rück; Prof. Dr. Horst Kunz 📂 Article 📅 1991 🏛 John Wiley and Sons 🌐 English ⚖ 351 KB 👁 1 views

and treated with lBuCl (1.18 g, 12.8 mmol) directly after filtration. The mixture was stirred at room temperature for 12 h before the orange solution was evaporated to dryness. Recrystallization of the residue from toluene (ca. 30 mL) affords a yellow crystalline powder (2.50 g, 40%). which decompos