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A Larger Scale Synthesis of a Natural Antibiotic, 2,4-Diacetylophloroglucinol (DAPG).

✍ Scribed by Jerzy Zakrzewski; Monika Karpinska; Zbigniew Malinski


Book ID
102005123
Publisher
John Wiley and Sons
Year
2007
Weight
15 KB
Volume
38
Category
Article
ISSN
0931-7597

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A Large Scale Synthesis of a Natural Ant
✍ Jerzy Zakrzewski; Monika KarpiΕ„ska; Zbigniew MaliΕ„ski πŸ“‚ Article πŸ“… 2007 πŸ› John Wiley and Sons 🌐 English βš– 230 KB πŸ‘ 1 views

## Abstract A natural antibiotic, 2,4‐diacetylophloroglucinol (DAPG), has been prepared by the acetylation of phloroglucinol (PhL) with acetic anhydride in the presence of boron trifluoride etherate complex. The crude DAPG is efficiently purified using chromatographic filtration with boiling eluent