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A handy preparation of bis(trimethylsilyl)methylamine

✍ Scribed by Jean-Paul Picard; Stéphane Grelier; Jacques Dunoquès; Jesus-Maria Aizpuna; Claudio Palomo


Book ID
103224400
Publisher
Elsevier Science
Year
1991
Tongue
English
Weight
212 KB
Volume
419
Category
Article
ISSN
0022-328X

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Preparation of bis-/2-chloroethyl-1,2-3H
✍ J. Filip 📂 Article 📅 1966 🏛 John Wiley and Sons 🌐 French ⚖ 232 KB

## Bis-(2-~hloroethy1-1,2-~H)methylamine hydrochloride was prepared, The starting product was a ~e t y l e n e -l , 2 -~H which was selectively hydrogenated to ethylene-1 ,2-3H. It was observed that on reduction with chromium ( I I ) chloride solution in dilute hydrochloric acid the isotopic exchang