A facile synthesis of 2,3-dicyanobutadiene-1,3 and 2,3-dicarbomethoxybutadiene-1,3
✍ Scribed by D. Belluš; C.D. Weis
- Publisher
- Elsevier Science
- Year
- 1973
- Tongue
- French
- Weight
- 115 KB
- Volume
- 14
- Category
- Article
- ISSN
- 0040-4039
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## Abstract The acid catalyzed reaction of glycerol‐d~5~ with bromoacetaldehyde dimethyl acetal affords the corresponding 2‐bromomethyl‐4‐hydroxymethyl‐1,3‐dioxolane, which was treated with lithium iodide in 2‐butanone to afford the pentadeuterated domiodol 1 in high isotopic purity.
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