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A facile stereospecific synthesis of α-hydrazino esters

✍ Scribed by Umut Oguz; Garett G. Guilbeau; Mark L. McLaughlin

Book ID: 104250776
Publisher: Elsevier Science
Year: 2002
Tongue: French
Weight: 68 KB
Volume: 43
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(02)00352-0

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✦ Synopsis

A convenient route to make a-hydrazino esters from their corresponding a-amino esters is reported. A key step is selective nitrosamine reduction using activated Zn, conc. HCl, and methanol at low temperatures giving nearly quantitative yields of the pure a-hydrazino esters

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