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A convenient synthesis of 1,3,6-dioxazocine, 1,3,7-dioxazonine, 1,3,8-dioxazecine and 1,3-dioxa-6,10-diazadodecane

✍ Scribed by Krzysztof E. Krakowiak; Barbara Kotelko; Jerald S. Bradshaw; N. Kent Dalley


Book ID
112129039
Publisher
Journal of Heterocyclic Chemistry
Year
1988
Tongue
English
Weight
323 KB
Volume
25
Category
Article
ISSN
0022-152X

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Synthesis of 1-pyrenyloxirane-3,6,8-3H1
✍ Daniel J. McCaustland; Alexander B. SusΓ n; James C. Wiley Jr. πŸ“‚ Article πŸ“… 1981 πŸ› John Wiley and Sons 🌐 French βš– 225 KB

## Abstract The syntheses of 1‐pyrenyloxirane‐3,6,8‐^3^H~1~, **7**, and its precursor, pyrene‐1,3,6,8‐^3^H~1~, **4**, are described. The synthesis pathway includes a novel preparation of **4** from 1‐pyrenyllithium and tritiated water in theoretical yield.