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Synthesis of 1-pyrenyloxirane-3,6,8-3H1

✍ Scribed by Daniel J. McCaustland; Alexander B. Susàn; James C. Wiley Jr.


Publisher
John Wiley and Sons
Year
1981
Tongue
French
Weight
225 KB
Volume
18
Category
Article
ISSN
0022-2135

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✦ Synopsis


Abstract

The syntheses of 1‐pyrenyloxirane‐3,6,8‐^3^H~1~, 7, and its precursor, pyrene‐1,3,6,8‐^3^H~1~, 4, are described. The synthesis pathway includes a novel preparation of 4 from 1‐pyrenyllithium and tritiated water in theoretical yield.


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