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A convenient family of chiral shift reagents for measurement of enantiomeric excesses of sulfoxides

✍ Scribed by M. Deshmukh; E. Duñach; S. Juge; H.B. Kagan

Publisher
Elsevier Science
Year
1984
Tongue
French
Weight
227 KB
Volume
25
Category
Article
ISSN
0040-4039

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Determination of enantiomeric purity of
Determination of enantiomeric purity of glycerides with a chiral PMR shift reagent
✍ J. Bus; C.M. Lok; A. Groenewegen 📂 Article 📅 1976 🏛 Elsevier Science 🌐 English ⚖ 518 KB

Tris(3-heptafluorobutyryl-d-camphorato)europium(Ill), Eu(hfbc) 3 was used to determine the optical purities of enantiomeric mixtures of tri-, di-and monoglycerides with various fatty acid chain lengths by proton magnetic resonance (PMR). Synthesized model enantiomers were used to assign PMR signals.