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A Concise Total Synthesis of the Lichen Macrolide (+)-Aspicilin

✍ Scribed by Dubost, Christophe; Markó, István E.; Ryckmans, Thomas

Book ID
120248023
Publisher
American Chemical Society
Year
2006
Tongue
English
Weight
86 KB
Volume
8
Category
Article
ISSN
1523-7060

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A Concise Total Synthesis of the Lichen
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## Abstract The asymmetric synthesis of the lichen macrolide (+)‐aspicilin (1) was realised in 19 steps and with high stereoselectivity (de ≥ 91 %, ee ≥ 96%). Three of the four stereogenic centres were generated by employing the SAMP/RAMP hydrazone method. Key steps of the synthesis are the α,α′‐do