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8,10-Dimethyl-2-keto-Δ 1,9;3,4 -hexahydronaphthalene: The Dienone-Phenol Rearrangement

✍ Scribed by Bloom, Stanley M.

Book ID
126121179
Publisher
American Chemical Society
Year
1958
Tongue
English
Weight
531 KB
Volume
80
Category
Article
ISSN
0002-7863

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The conversion of 2-formyl-3-keto-9-methyl-Δ1,4-hexahydronaphthalene into a perhydroazulene derivative
✍ Drury Caine; John F. DeBardeleben Jr.; School of Chemistry 📂 Article 📅 1965 🏛 Elsevier Science 🌐 French ⚖ 247 KB

We have found that on irradiation in aqueous acetic acid followed by base catalyzed defomylatlon of the c-de photo-product, the 2-fonqyl dienone III is converted into the5/7-fused dienone IV in 7% overall yield. Ccmpound III was prepared from the octalone I (1) by a procedure similar to that employ