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615. Deoxynucleosides and related compounds. Part VI. The synthesis of 2-thiouridine and of 3′-deoxyuridine

✍ Scribed by Brown, D. M. ;Parihar, D. B. ;Todd, Alexander ;Varadarajan, S.

Book ID
118740889
Publisher
The Royal Society of Chemistry
Year
1958
Weight
740 KB
Volume
0
Category
Article
ISSN
0368-1769

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✍ C.-Y. Shiue; A. P. Wolf; D. N. Slatkin 📂 Article 📅 1980 🏛 John Wiley and Sons 🌐 French ⚖ 289 KB

## Abstract Thymine‐α,α,α‐d~3~ (**4**) was synthesized from perdeuterated methyl iodide and pyrimidine‐lithium. Thymidine‐α,α,α‐d~3~ (**8**) was then synthesized by coupling compound **4** with 1α‐chloro‐2‐deoxy‐3,5‐bis(p‐toluoyl)‐α‐D‐ribofuranosyl chloride in the presence of Friedal‐Crafts catalys