The asymmetric unit of the title compound, C 16 H 13 ClN 4 O, contains two crystallographically independent molecules, A and B. The pyrazole ring of A makes dihedral angles of 5.8 (1) and 7.2 (1) with the pyrimidine ring and the benzene ring, respectively; the corresponding values in molecule B are
6-Nitro-1,3-benzodioxole-4-carbaldehyde
✍ Scribed by Hussain, Mukhtiar ;Ali, Saqib ;Altaf, Muhammad ;Stoeckli-Evans, Helen
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 275 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
No coin nor oath required. For personal study only.
📜 SIMILAR VOLUMES
In the title structure, C 16 H 12 N 4 O 3 Á0.5H 2 O, the uncoordinated water molecule lies on a special position of site symmetry 2; O-HÁ Á ÁO and N-HÁ Á ÁO hydrogen bonds link the water and organic molecules into a layer structure.
In the title compound, C 16 H 11 ClO 6 , the dihedral angle between the two benzene rings is 86.9 (3) .
The title compound, C 16 H 13 BrO 6 , was synthesized in an anhydrous medium. The methylenedioxobenzoate moiety and the methoxyphenyl fragment form a dihedral angle of 65.06 (8) .