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Methyl 7-(4-chloro­benzo­yloxy)-1,3-benzodioxole-5-carboxyl­ate

✍ Scribed by Hu, Zhi-Qiang ;Zheng, Lei ;Li, Chang-Jin ;Chang, Jun-Biao

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
99 KB
Volume
63
Category
Article
ISSN
1600-5368

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✦ Synopsis

In the title compound, C 16 H 11 ClO 6 , the dihedral angle between the two benzene rings is 86.9 (3) .

📜 SIMILAR VOLUMES

4-Methoxy­phenyl 4-bromo-7-methoxy-1,3-b
4-Methoxy­phenyl 4-bromo-7-methoxy-1,3-benzodioxole-5-carboxyl­ate
✍ Zheng, Lei ;Zheng, Xiu-Fang ;Zhang, Dan ;Chang, Jun-Biao 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 138 KB

The title compound, C 16 H 13 BrO 6 , was synthesized in an anhydrous medium. The methylenedioxobenzoate moiety and the methoxyphenyl fragment form a dihedral angle of 65.06 (8) .

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Single-crystal X-ray study T = 160 K Mean '(C±C) = 0.002 A Ê R factor = 0.041 wR factor = 0.116 Data-to-parameter ratio = 21.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê Disorder in main residue R factor = 0.061 wR factor = 0.208 Data-to-parameter ratio = 14.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.