## Abstract A new and convenient synthesis of a variety of __N__‐ and __S__‐substituted tetrazoles has been developed via azide and Mannich reaction methods. Compounds were characterized by elemental analysis, MALDI MS, and ^1^H NMR data. © 2007 Wiley Periodicals, Inc. Heteroatom Chem 18:637–643, 2
✦ LIBER ✦
5,5′-Dithiobis(1-phenyl-1H-tetrazole)
✍ Scribed by Brito, Iván ;Cárdenas, Alejandro ;Mundaca, Aldo ;Villalobos, Hada ;López-Rodríguez, Matías
- Publisher
- International Union of Crystallography
- Year
- 2007
- Tongue
- English
- Weight
- 293 KB
- Volume
- 63
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
The structure of the title compound, C 14 H 10 N 8 S 2 , comprises two 1-phenyl-1H-tetrazole-5-thiolate units linked by an S-S disulfide bridge. The C-S-S-C torsion angle is 81.9 (1) . C-HÁ Á ÁN hydrogen bonding, with CÁ Á ÁN = 3.413 (4) A ˚and C-HÁ Á ÁN = 147 , link the molecules into supramolecular chains in the crystal structure.
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