1,4-Bis(1-phenyl-1H-tetrazol-5-ylsulfanyl)butane
✍ Scribed by Wang, Wei ;Liu, Hui-Min ;Zhang, Wen-Qin
- Publisher
- International Union of Crystallography
- Year
- 2005
- Tongue
- English
- Weight
- 131 KB
- Volume
- 61
- Category
- Article
- ISSN
- 1600-5368
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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê R factor = 0.049 wR factor = 0.110 Data-to-parameter ratio = 15.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, C 20 H 22 N 8 O 2 S 2 , contains a center of inversion at the mid-point of the central C-C bond. The mean planes of the phenyl and the 1H-tetrazol-5-ylsulfanyl rings make a dihedral angle of 53.95 (16) .
The molecule of the title compound, C 10 H 18 N 8 S 2 , lies on a twofold rotation axis. Methyl C atoms contact N atoms of adjacent molecules through C-HÁ Á ÁN hydrogen bonds [3.445 (3) A ˚] in a molecular layer. In addition, the layers are linked by weak SÁ Á ÁS interactions [3.636 (3) A ˚].