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525. Oxidation of alkoxyphenols. Part IV. 4-Methoxy-2,5-di-t-butylphenol

✍ Scribed by Hewgill, F. R. ;Kennedy, B. R.

Book ID: 121393982
Publisher: The Royal Society of Chemistry
Year: 1965
Weight: 424 KB
Category: Article
ISSN: 0368-1769
DOI: 10.1039/JR9650002921

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The initial yield of 3,5-di-t-butylsalicylic acid obtained via Kolbe-Schmitt carboxylation of the potassium salt of 2,4-di-t-butylphenol was less than 1% and was accompanied by a 65% yield of 2,2'-dihydroxy-3,3',5,5'- tetra-t-butylbiphenyl, a dimer of the 2,4-di-t-butylphenol formed by ortho couplin