5-tert-Butyl-2-(N,N-dimethylaminocarbonylthio)isophthalaldehyde
✍ Scribed by McKenzie, Christine ;Bond, Andrew D.
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 232 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
No coin nor oath required. For personal study only.
✦ Synopsis
Single-crystal X-ray study T = 180 K Mean '(C±C) = 0.002 A Ê R factor = 0.037 wR factor = 0.112 Data-to-parameter ratio = 25.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
The title compound [Li~2~(C~11~H~26~N~3~)~2~], is a dimer chelate complex and features a planar Li~2~N~2~ ring with an Li...Li distance of 2.449 (3) Å and a bicyclic ring system. The coordination geometry of both Li atoms is distorted tetrahedral, each Li unit being surrounded by two amide and two a
The molecule of the title compound, C 22 H 29 NOS, is nonplanar, with a dihedral angle of 32.06 (9) between the two aromatic rings.
The title compound, C 27 H 39 N 3 O 9 , is a key intermediate in the synthesis of novel -turn mimetics based on electrophilic amination of enantiomerically pure (S)-pyroglutamic acid. The molecule adopts an extended conformation which is not stabilized by either intra-or intermolecular hydrogen bond