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[(1-tert-Butyl-2-phenyl­vinyl­amino)(di­methyl­amino)­di­methyl­silyl-κ2N,N′] (N,N,N′,N′-tetra­methyl­enedi­amine-κ2N,N′)­lithium(I)

✍ Scribed by Shi, He-Ping ;Liu, Dian-Sheng ;Huang, Shu-Ping

Publisher
International Union of Crystallography
Year
2003
Tongue
English
Weight
211 KB
Volume
59
Category
Article
ISSN
1600-5368

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✍ Shi, He-Ping ;Liu, Dian-Sheng ;Huang, Shu-Ping 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 167 KB

Single-crystal X-ray study T = 183 K Mean '(C±C) = 0.008 A Ê R factor = 0.076 wR factor = 0.104 Data-to-parameter ratio = 16.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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In the title compound, [Ni(C 16 H 16 N 3 O 2 ) 2 ]ÁC 2 H 6 OS, the Ni II atom lies on a crystallographic centre of symmetry and its coordination geometry is distorted square-planar, involving four N atoms from two oxime ligands. The dimethyl sulfoxide solvent is disordered over a crystallographic tw