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4,5-Bis(phenyl­sulfonyl­thio)-1,3-dithiol­ane-2-thione

✍ Scribed by Wang, Yan-Ling ;Yu, Wen-Tao ;Xu, Dong ;Wang, Xin-Qiang ;Zhang, Guang-Hui ;Feng, Lin


Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
382 KB
Volume
61
Category
Article
ISSN
1600-5368

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In the crystal structure of the title compound, C 7 H 10 O 2 S 5 , weak intermolecular SÁ Á ÁS interactions and strong intra-and intermolecular O-HÁ Á ÁO hydrogen bonds link the molecules, forming a three-dimensional supramolecular architecture.

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The electron impact ionization mass spectra of 4,5-bis(alkylthio)-l,3dithiole-2-thiones and their 1,'tdithiole-3thione isomers were studied by accurate mass measurements and linked scans. The relative abundance of ions formed following the extrusion of S, , CS or CS, allows an unambiguous isomer dif