4,5-Bis(phenylsulfonylthio)-1,3-dithiolane-2-thione
✍ Scribed by Wang, Yan-Ling ;Yu, Wen-Tao ;Xu, Dong ;Wang, Xin-Qiang ;Zhang, Guang-Hui ;Feng, Lin
- Publisher
- International Union of Crystallography
- Year
- 2005
- Tongue
- English
- Weight
- 382 KB
- Volume
- 61
- Category
- Article
- ISSN
- 1600-5368
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free from isotetrasilane). Results of determinations with isotetrasilane will be published later. Combustion in a calorimetric bomb is suitable for disilane, which is readily condensed, and for tri-and tetrasilanes, which are liquids [4]. On account of its low b.p. (-1 11.6 "C), however, SiH4 could
In the crystal structure of the title compound, C 7 H 10 O 2 S 5 , weak intermolecular SÁ Á ÁS interactions and strong intra-and intermolecular O-HÁ Á ÁO hydrogen bonds link the molecules, forming a three-dimensional supramolecular architecture.
The electron impact ionization mass spectra of 4,5-bis(alkylthio)-l,3dithiole-2-thiones and their 1,'tdithiole-3thione isomers were studied by accurate mass measurements and linked scans. The relative abundance of ions formed following the extrusion of S, , CS or CS, allows an unambiguous isomer dif