4,5-Bis(2-hydroxyethylsulfanyl)-1,3-dithiole-2-thione
✍ Scribed by Hu, Pu-Zhou ;Qin, Jian-Hua ;Chen, Jun-Qing ;Wang, Lu ;Zhao, Bang-Tun
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 433 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
No coin nor oath required. For personal study only.
✦ Synopsis
In the crystal structure of the title compound, C 7 H 10 O 2 S 5 , weak intermolecular SÁ Á ÁS interactions and strong intra-and intermolecular O-HÁ Á ÁO hydrogen bonds link the molecules, forming a three-dimensional supramolecular architecture.
📜 SIMILAR VOLUMES
In the title compound, C 19 H 17 O 3 N 4 S, a substituted oxadiazole derivative and an important biologically active compound, electron delocalization in the oxadiazole ring is reflected in the C-N bond lengths.
The crystal structure of the title compound, C 14 H 14 N 2 S 8 , at 180 K contains pairs of molecules related by centres of inversion, arranged in a herringbone-type manner to form layers. NÁ Á Á\*(S-C) interactions exist between layers.
The electron impact ionization mass spectra of 4,5-bis(alkylthio)-l,3dithiole-2-thiones and their 1,'tdithiole-3thione isomers were studied by accurate mass measurements and linked scans. The relative abundance of ions formed following the extrusion of S, , CS or CS, allows an unambiguous isomer dif