1,3-Dithiolane-2-thione-4,5-dione

✍ Scribed by Dipl.-Chem. B. Krebs; Doz. Dr. G. Gattow

• Publisher: John Wiley and Sons
• Year: 1963
• Tongue: English
• Weight: 137 KB
• Volume: 2
• Category: Article
• ISSN: 0044-8249
• DOI: 10.1002/anie.196306182

✦ Synopsis

free from isotetrasilane). Results of determinations with isotetrasilane will be published later. Combustion in a calorimetric bomb is suitable for disilane, which is readily condensed, and for tri-and tetrasilanes, which are liquids [4]. On account of its low b.p. (-1 11.6 "C), however, SiH4 could only be burnt at constant pressure in a specially designed combustion chamber [5]. This method was also applied to d i s i 1 an e .