free from isotetrasilane). Results of determinations with isotetrasilane will be published later. Combustion in a calorimetric bomb is suitable for disilane, which is readily condensed, and for tri-and tetrasilanes, which are liquids [4]. On account of its low b.p. (-1 11.6 "C), however, SiH4 could
✦ LIBER ✦
Strukturberichtigung - 5-Methylen-thiazolidin-2-thione statt 3,4-Dihydro-1,3-thiazin-2-thione
✍ Scribed by Wolfgang Hanefeld; Martin Schlitzer; Joachim v. Gösseln
- Publisher
- John Wiley and Sons
- Year
- 1985
- Tongue
- English
- Weight
- 156 KB
- Volume
- 318
- Category
- Article
- ISSN
- 0365-6233
No coin nor oath required. For personal study only.
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The title compound (C 15 H 12 N 3 OSCl) crystallizes in the monoclinic space group P2 1 /n with a = 11.211( 3), b = 8.106(2), c = 17.494(4) Å, β = 104.49(2)º, V = 1539.2(7) Å 3 , Z = 4, D cal = 1.371 Mg/m 3 at T = 293 K. The structure was solved by direct methods and refined by full-matrix least-squ