𝔖 Bobbio Scriptorium
✦   LIBER   ✦

4-tert-Butyl-2-(4-pyridyl)-N,N′-bis­(tri­methyl­silyl)­propane-1,3-di­imine

✍ Scribed by Chen, Xia ;Wang, Li ;Huang, Shu-Ping ;Liu, Dian-Sheng

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
417 KB
Volume
60
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis

In the title compound, C 18 H 33 N 3 Si 2 , the central diketiminate system is essentially planar. A short intramolecular hydrogen bond involving the imine N atoms forms a pseudo-sixmembered ring.

📜 SIMILAR VOLUMES

{4,4′-Di-tert-butyl-6,6′-bis­(di­methoxy
{4,4′-Di-tert-butyl-6,6′-bis­(di­methoxy­methyl)-2,2′-[propane-1,3-diyl­bis­(nitrilo­methyl­idyne)]­bis­(thio­phenolato)-κ4S,N,N′,S′}nickel(II)
✍ Bjernemose, Jens K. ;McKenzie, Christine J. ;Raithby, Paul R. ;Teat, Simon J. 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 375 KB

Single-crystal synchrotron study T = 150 K Mean '(C±C) = 0.004 A Ê R factor = 0.084 wR factor = 0.228 Data-to-parameter ratio = 53.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

(1R,2R)-1,3-Bis(tert-butyl­di­methyl­sil
(1R,2R)-1,3-Bis(tert-butyl­di­methyl­silyl­oxy)-2-(4-hydroxy­butan­amido)-1-(4-nitro­phenyl)­propane
✍ Johansson, Dorte ;Larsen, Frank B. ;Bond, Andrew D. ;Nielsen, Poul 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 386 KB

Single-crystal X-ray study T = 180 K Mean '(C±C) = 0.012 A Ê Disorder in main residue R factor = 0.056 wR factor = 0.148 Data-to-parameter ratio = 6.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.