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(1R,2R)-1,3-Bis(tert-butyl­di­methyl­silyl­oxy)-2-(4-hydroxy­butan­amido)-1-(4-nitro­phenyl)­propane

✍ Scribed by Johansson, Dorte ;Larsen, Frank B. ;Bond, Andrew D. ;Nielsen, Poul

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
386 KB
Volume
60
Category
Article
ISSN
1600-5368

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✦ Synopsis

Single-crystal X-ray study T = 180 K Mean '(C±C) = 0.012 A Ê Disorder in main residue R factor = 0.056 wR factor = 0.148 Data-to-parameter ratio = 6.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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The crystal structure of the title compound, C~36~H~40~N~2~O~2~, has been determined at 173 (2) K. The molecule has __C__ ~2~ symmetry and the asymmetric unit contains one half-molecule. An intramolecular O—H...N hydrogen bond is formed between the phenol OH group and the Schiff base N atom.