In the structure of the title compound, C~15~H~13~ClN~2~OS, the dihedral angle between the two aromatic ring planes is 30.46 (8)°. Intermolecular N—H...S hydrogen bonds link the molecules into dimeric units which are stacked along [010].
4-(Benzo[b]thiophen-3-yl)-1-methylpiperidine-4-carbonitrile
✍ Scribed by Sonar, Vijayakumar N. ;Parkin, Sean ;Crooks, Peter A.
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 238 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
No coin nor oath required. For personal study only.
✦ Synopsis
Single-crystal X-ray study T = 90 K Mean '(C±C) = 0.004 A Ê R factor = 0.044 wR factor = 0.098 Data-to-parameter ratio = 13.7
For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
In the structure of the title compound, C~16~H~16~N~2~OS, the dihedral angle between the two aromatic ring planes is 68.08 (9)°. Intermolecular N—H...S hydrogen bonds link the molecules into dimeric units which are stacked along [100].
The title compound, C 14 H 8 Cl 4 N 2 OS, shows the typical geometric parameters of substituted thiourea derivatives. The dihedral angle formed by the two benzene ring planes is 38.39 (7) . The crystal packing is characterized by N-HÁ Á ÁO and N-HÁ Á ÁS hydrogen bonds.
The title compound, C 6 H 6 N 2 S, consists of a thiophene ring carrying three substitutent groups. Two NÐHÁ Á ÁN intermolecular hydrogen bonds link neighboring molecules into a threedimensional network.
The benzoyl and methoxybenzene groups in the title compound, C 16 H 16 N 2 O 2 S, are cis and trans, respectively, with respect to the C S bond. The crystal packing is characterized by N-HÁ Á ÁO and N-HÁ Á ÁS hydrogen bonds.