4-Acetyl-N,N-dibenzoylphenylamine
✍ Scribed by Usman, Anwar ;Razak, Ibrahim Abdul ;Fun, Hoong-Kun ;Chantrapromma, Suchada ;Tian, Jing-Zhi ;Zhang, Yan ;Xu, Jian-Hua
- Publisher
- International Union of Crystallography
- Year
- 2002
- Tongue
- English
- Weight
- 341 KB
- Volume
- 58
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 183 K Mean '(C±C) = 0.002 A Ê R factor = 0.054 wR factor = 0.135 Data-to-parameter ratio = 14.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
N-benzoyl and 4-acetylaniline moieties are coplanar. The aromatic ring of the other benzoyl is twisted with respect to the attached 4-acetylaniline. The molecular structure is maintained by intramolecular CÐHÁ Á ÁO and NÐHÁ Á ÁO interactions, and the packing is stabilized by a weak CÐ HÁ Á ÁO intera
The title complex, C 21 H 21 N, crystallizes in space group P1, with Z = 6. The N atom is sp 2 -hybridized. The geometry of each of the three independent molecules is unremarkable. The interaction of the three molecules is discussed.
Single-crystal X-ray study T = 273 K Mean '(C±C) = 0.003 A Ê R factor = 0.043 wR factor = 0.116 Data-to-parameter ratio = 11.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 183 K Mean '(C±C) = 0.004 A Ê R factor = 0.054 wR factor = 0.131 Data-to-parameter ratio = 13.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.