N′-(4-Chlorobenzoyl)-N,N-diphenylthiourea
✍ Scribed by Arslan, Hakan ;Flörke, Ulrich ;Külcü, Nevzat
- Publisher
- International Union of Crystallography
- Year
- 2003
- Tongue
- English
- Weight
- 320 KB
- Volume
- 59
- Category
- Article
- ISSN
- 1600-5368
No coin nor oath required. For personal study only.
📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê R factor = 0.045 wR factor = 0.125 Data-to-parameter ratio = 17.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Molecules of the title compound, C 16 H 16 N 2 O 3 S, are linked by N-HÁ Á ÁS hydrogen bonds to form centrosymmetric dimers [NÁ Á ÁS = 3.4501 (13) A ˚]. The N 0 -phenyl and N-phenyl rings are twisted by 52.7 (1) and 23.3 (1) , respectively, from the essentially planar -NHC( S)NC( O)-moiety.
Single-crystal X-ray study T = 213 K Mean '(C±C) = 0.004 A Ê R factor = 0.053 wR factor = 0.148 Data-to-parameter ratio = 16.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 150 K Mean '(C±C) = 0.003 A Ê R factor = 0.033 wR factor = 0.081 Data-to-parameter ratio = 13.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.