𝔖 Bobbio Scriptorium
✦   LIBER   ✦

N-(4-Methoxy­benzoyl)-N′-(4-methoxy­phenyl)­thio­urea

✍ Scribed by Ali, Hapipah M. ;Abdul Halim, Siti Nadiah ;Basirun, Wan Jefri ;Ng, Seik Weng

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
110 KB
Volume
61
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis

Molecules of the title compound, C 16 H 16 N 2 O 3 S, are linked by N-HÁ Á ÁS hydrogen bonds to form centrosymmetric dimers [NÁ Á ÁS = 3.4501 (13) A ˚]. The N 0 -phenyl and N-phenyl rings are twisted by 52.7 (1) and 23.3 (1) , respectively, from the essentially planar -NHC( S)NC( O)-moiety.

📜 SIMILAR VOLUMES

N-(p-Methoxy­benzoyl)-N′-(o-methoxy­phen
N-(p-Methoxy­benzoyl)-N′-(o-methoxy­phenyl)­thio­urea
✍ Ali, Hapipah ;Halim, S. Nadiah A. ;Khamis, Nur Ashikin ;Yusof, M. Sukeri ;Yamin, 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 355 KB

Single-crystal X-ray study T = 273 K Mean '(C±C) = 0.002 A Ê R factor = 0.039 wR factor = 0.105 Data-to-parameter ratio = 15.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

N-(4-Methoxy­benzoyl)-N'-o-tolyl­thio­ur
N-(4-Methoxy­benzoyl)-N'-o-tolyl­thio­urea
✍ Yusof, M. Sukeri M. ;Yamin, Bohari M. 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 235 KB

Single-crystal X-ray study T = 273 K Mean '(C±C) = 0.002 A Ê R factor = 0.038 wR factor = 0.110 Data-to-parameter ratio = 15.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

N-(4-Methoxy­phen­yl)thio­urea
N-(4-Methoxy­phen­yl)thio­urea
✍ Teh, Jeannie Bee-Jan ;Karthikeyan, Mari Sithambaram ;Fun, Hoong-Kun ;Patil, P. S 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 211 KB

In the title compound, C 8 H 10 N 2 OS, the dihedral angle between the benzene ring and the thiourea group is 59.23 (4) . Molecules are linked via N-HÁ Á ÁO/S hydrogen bonds, forming a two-dimensional network.