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N-[3-(Hydro­xy­methyl)­phenyl]-N′-(4-methoxy­benzoyl)­thio­urea

✍ Scribed by Ngah, Nurziana ;Fauzi, Noor Fadzlina Mohd ;Yamin, Bohari M.

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
182 KB
Volume
61
Category
Article
ISSN
1600-5368

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Molecules of the title compound, C 16 H 16 N 2 O 3 S, are linked by N-HÁ Á ÁS hydrogen bonds to form centrosymmetric dimers [NÁ Á ÁS = 3.4501 (13) A ˚]. The N 0 -phenyl and N-phenyl rings are twisted by 52.7 (1) and 23.3 (1) , respectively, from the essentially planar -NHC( S)NC( O)-moiety.

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Single-crystal X-ray study T = 273 K Mean '(C±C) = 0.002 A Ê R factor = 0.039 wR factor = 0.105 Data-to-parameter ratio = 15.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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Single-crystal X-ray study T = 213 K Mean '(C±C) = 0.004 A Ê R factor = 0.053 wR factor = 0.148 Data-to-parameter ratio = 16.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.