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4′-(4-Chloro­phenyl)-3′'-ethyl-1′-methyl-1H-indole-3-spiro-2′-pyrrolidine-3′-spiro-5′′-[1,3]­thia­zole-2(3H),2′′(3′′H),4′′(5′′H)-trione benzene sesquisolvate

✍ Scribed by Li, Xiao-Fang ;Feng, Ya-Qing ;Shi, Da-Xin ;Chen, Hong-Liang

Publisher
International Union of Crystallography
Year
2003
Tongue
English
Weight
170 KB
Volume
59
Category
Article
ISSN
1600-5368

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê Disorder in main residue R factor = 0.047 wR factor = 0.119 Data-to-parameter ratio = 13.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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In the title compound, C 43 H 36 Cl 2 N 4 O 3 Á0.5C 6 H 6 , there exists a trispiro ring system, which consists of a planar 2-oxindole ring, an envelope pyrrolidine ring, an envelope isoxazoline ring and a boat-shaped piperidone ring. The crystal structure is stabilized by NÐHÁ Á ÁN intermolecular i

1-Methyl-4′-(3-nitro­phenyl)-1H-indole-3
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✍ Seshadri, P. R. ;Selvanayagam, S. ;Velmurugan, D. ;Ravikumar, K. ;Sureshbabu, A. 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 237 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê R factor = 0.052 wR factor = 0.163 Data-to-parameter ratio = 15.5 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

4′-(4-Chloro­phenyl)-1′-methyl-4′′,5′′,6
4′-(4-Chloro­phenyl)-1′-methyl-4′′,5′′,6′′,7′′-tetra­hydro-1H-indole-3-spiro-2′-pyrrolidine-3′-spiro-2′′-(thia­zolo­[3,2-a]­pyrimidine)-2(3H),3′′(2′′H)-dione
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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê R factor = 0.061 wR factor = 0.170 Data-to-parameter ratio = 16.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.