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1′-Methyl-4′-tolyl-1H-indole-3-spiro-2′-pyrrolidine-3′-spiro-5′′-(thia­zolo­[3,2-b][1,2,4]­triazole)-2,6′′(3H,5′′H)-dione

✍ Scribed by Li, Xiao-Fang ;Feng, Ya-Qing ;Gao, Bo ;Yao, Guang-Yuan

Publisher
International Union of Crystallography
Year
2003
Tongue
English
Weight
133 KB
Volume
59
Category
Article
ISSN
1600-5368

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê Disorder in main residue R factor = 0.047 wR factor = 0.119 Data-to-parameter ratio = 13.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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In the title compound, C~30~H~22~N~4~O~2~S, two spiro junctions link a planar 2-oxoindole ring, a pyrrolidine ring and a thiazolo[3,2-__a__][1,3]benzimidazol-3-one system. Molecules form dimers connected by N—H...N hydrogen bonds.

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê R factor = 0.048 wR factor = 0.113 Data-to-parameter ratio = 15.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

4′-(4-Chloro­phenyl)-1′-methyl-4′′,5′′,6
4′-(4-Chloro­phenyl)-1′-methyl-4′′,5′′,6′′,7′′-tetra­hydro-1H-indole-3-spiro-2′-pyrrolidine-3′-spiro-2′′-(thia­zolo­[3,2-a]­pyrimidine)-2(3H),3′′(2′′H)-dione
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