𝔖 Bobbio Scriptorium
✦   LIBER   ✦

1′-Benzyl-3-(2,6-di­chloro­phenyl)-1′′-methyl-4,4′′-di­phenyl­oxazole-5(4H)-spiro-3′-piperidine-5′-spiro-3′′-pyrrolidine-2′′-spiro-3′′′-1H-indole-2′′′(3′′′H),4′-dione benzene hemisolvate

✍ Scribed by Li, Xiao-Fang ;Feng, Ya-Qing ;Hu, Xiao-Fen ;Xu, Mian

Publisher
International Union of Crystallography
Year
2003
Tongue
English
Weight
170 KB
Volume
59
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis

In the title compound, C 43 H 36 Cl 2 N 4 O 3 Á0.5C 6 H 6 , there exists a trispiro ring system, which consists of a planar 2-oxindole ring, an envelope pyrrolidine ring, an envelope isoxazoline ring and a boat-shaped piperidone ring. The crystal structure is stabilized by NÐHÁ Á ÁN intermolecular interactions.

📜 SIMILAR VOLUMES

1′-Methyl-4′-(2,4-di­chloro­phenyl)-1H-i
1′-Methyl-4′-(2,4-di­chloro­phenyl)-1H-indole-3-spiro-2′-pyrrolidine-3′-spiro-5′′-(thia­zolo­[3,2-b][1,2,4]­triazole)-2,6′′(3H,5′′H)-dione
✍ Li, Xiao-Fang ;Feng, Ya-Qing ;Yao, Guang-Yuan ;You, Xu-Dong 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 223 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê Disorder in main residue R factor = 0.047 wR factor = 0.119 Data-to-parameter ratio = 13.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

1′-Methyl-2′′-phenyl­cyclo­hexane-1-spir
1′-Methyl-2′′-phenyl­cyclo­hexane-1-spiro-4′-[acenaphthene-1-spiro-2′-pyrrolidine-3′-spiro-4′′(5′′H)-[1,3]­oxazole]-2,5′′-dione
✍ Selvanayagam, S. ;Velmurugan, D. ;Ravikumar, K. ;Jayashankaran, J. ;Durga, R. Ra 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 259 KB

In the title compound, C 29 H 26 N 2 O 3 , the pyrrolidine ring adopts an envelope conformation and the cyclohexane ring adopts a chair conformation. The structure is stabilized by intramolecular CÐHÁ Á ÁO and %±% interactions.