A method for spatially three-dimensional (3D) localized twodimensional (2D) 1 H-13 C correlation spectroscopy, localized HSQC, is proposed. This method has the following special feature in the preparation period. The 180Β°( 13 C) and 180Β°( 1 H) pulses are separated in time, and the 180Β°( 13 C) pulse
3D H, C, P correlation: A new application of 3D NMR spectroscopy
β Scribed by Stefan Berger; Peter Bast
- Publisher
- John Wiley and Sons
- Year
- 1993
- Tongue
- English
- Weight
- 200 KB
- Volume
- 31
- Category
- Article
- ISSN
- 0749-1581
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β¦ Synopsis
Abstract
The first example of 3D NMR spectroscopy involving ^1^H, ^13^C and ^31^P nuclei is described. The use of this technique for difficult signal assignments in organophosphorus chemistry is demonstrated.
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