## Abstract Twenty‐six new aminoflavones have been synthesised by two different methods and the structure elucidation was accomplished using extensive 1D (^1^H, ^13^C) and 2D NMR spectroscopic studies (COSY, HSQC and HMBC experiments). Copyright © 2006 John Wiley & Sons, Ltd.
Synthesis and structure elucidation of five new pyrimido[5,4-c]quinoline-4(3H)-one derivatives using 1D and 2D NMR spectroscopy
✍ Scribed by Yong Ai; Guangzhong Yang; Jianchao Liu; Yu Chen; Lu Liu; Xinxiang Lei
- Publisher
- John Wiley and Sons
- Year
- 2010
- Tongue
- English
- Weight
- 129 KB
- Volume
- 48
- Category
- Article
- ISSN
- 0749-1581
- DOI
- 10.1002/mrc.2689
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✦ Synopsis
Abstract
Five new 2‐(amino/aroxy)‐5‐methylpyrimido[5,4‐c]quinolin‐4(3__H__)‐one derivatives have been designed and synthesized via an aza‐Wittig reaction, and the structure elucidation was accomplished using extensive 1D (^1^H, ^13^C) and 2D NMR spectroscopic studies (COSY, HSQC and HMBC experiments). Copyright © 2010 John Wiley & Sons, Ltd.
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Regioselective synthesis of 2‐[1‐(2‐oxo‐2‐phenylethyl)‐1__H__‐[1,2,3]triazol‐4‐ylmethoxy]‐benzaldehyde derivatives was achieved by [3 + 2] cycloaddition reaction of 2‐(prop)‐2‐ynyloxy‐benzaldehyde derivatives with phenacyl azide. The regiochemistry and the spectral assignments of the synthesized tri
## Abstract For Abstract see ChemInform Abstract in Full Text.
## Abstract A series of new 1__H__‐pyrazolo[3,4‐__d__]pyrimidin‐4(__5H__)‐one Derivatives **5** has been designed and regio‐selectively synthesized __via__ a tandem aza‐Wittig reaction. The structures of all compounds prepared have been confirmed by ^1^H NMR, IR, EI‐MS spectroscopy and elemental an