31P NMR chemical shielding tensors of diethyl [5,6-dichloro-1,3-benzodioxol-(2)] phosphonate
β Scribed by J. Rohonczy; F. Ermark; U. Haeberlen; G. Klose; M. Schulz
- Book ID
- 107735133
- Publisher
- Elsevier Science
- Year
- 1991
- Tongue
- English
- Weight
- 375 KB
- Volume
- 180
- Category
- Article
- ISSN
- 0009-2614
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Static and MAS 31P NhlR spectra of polycrystalline h-PqOre and phosphates KsP04, KaP207, KsPsOre, KsPsOs and (KPOs), were measured at 109.3 MHz. It is shown that the principal values of the 31P shielding tensor and the isotropic 31P chemical shift values reflect sensitively the constitution of both
## Abstract The spectral analyses and syntheses of several novel 2,10βdichloroβ6βaryloxy/alkylβ12__H__βdibenzo [__d__,__g__] [1,3,2] dioxaphosphocin 6βoxides have been achieved. Longβrange coupling [^5^__J__(H,P) = 2.4 Hz] was observed between phosphorus and the bridged methylene protons. Based upo