A facile synthesis and spectral (ir, 1H, 13C, 31P nmr) studies of 2,10-dichloro-6-aryloxy-12H-dibenzo[d,g][1,3,2]dioxaphosphocin 6-sulfides
✍ Scribed by C. Devendranath Reddy; P. Mallikarjuna Reddy; D. Ramasubba Reddy; M. Nagalakshmamma; K. Anuradha; C. Naga Raju; K. Darrell Berlin; Kevin M. Couch; Sameer Tyagi
- Book ID
- 112131355
- Publisher
- Journal of Heterocyclic Chemistry
- Year
- 1995
- Tongue
- English
- Weight
- 358 KB
- Volume
- 32
- Category
- Article
- ISSN
- 0022-152X
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## Abstract The spectral analyses and syntheses of several novel 2,10‐dichloro‐6‐aryloxy/alkyl‐12__H__‐dibenzo [__d__,__g__] [1,3,2] dioxaphosphocin 6‐oxides have been achieved. Long‐range coupling [^5^__J__(H,P) = 2.4 Hz] was observed between phosphorus and the bridged methylene protons. Based upo
## Abstract Synthesis of several novel 6‐aryloxy/arylmio/chloroethoxy‐2,10‐dichloro‐4,8‐dinitro‐12‐trichloro‐memyl‐12__H__‐dibenzo[__d,g__][1,3,2]dioxaphosphocin 6‐oxides (**4a‐k**) was accomplished by reacting 2,2‐bis (2‐hydroxy‐5‐chloro‐3‐nitrophenyl)‐1,1,1‐trichloroethane **2** with different ar