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3-Chloro-1-phenyl­sulfonyl-1H-indole-2-carbaldehyde

✍ Scribed by Palani, K. ;Ponnuswamy, M. N. ;Jaisankar, P. ;Srinivasan, P. C. ;Nethaji, M.

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
208 KB
Volume
62
Category
Article
ISSN
1600-5368

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In the title compound, C~21~H~15~NO~3~S~2~, the phenyl ring of the phenylsulfonyl substituent makes a dihedral angle of 73.6 (1)° with the mean plane of the indole ring system, whereas the phenyl ring of the phenylsulfanyl group forms a dihedral angle of 73.9 (1)° with the mean plane of the indole r

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To a stirred solution of aluminium chloride (20 mmol) in dry tetrahydrofuran (100 ml), sodium azide (60 mmol) and 1-phenylsulfonyl-

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In the title structure, C 16 H 10 N 2 O 3 S, there are two crystallographically independent molecules in the asymmetric unit. In one molecule, the dihedral angle between the indole ring system and the phenyl ring is 68.3 (2) , and in the other it is 80.3 (2) . C-HÁ Á ÁO, C-HÁ Á ÁN and C-HÁ Á Á inter

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In the title molecule, C 21 H 17 NO 3 S 2 , the sulfonyl-bound and sulfinyl-bound phenyl rings form dihedral angles of 82.04 (5) and 26.26 (8) , respectively, with the indole ring system. In the crystal structure C-HÁ Á ÁO, C-HÁ Á Á andinteractions form a two-dimensional network.