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3, 6-endoxocyclohexanes and -cyclohexenes. XXV. Some reactions of dimethyl 4,5-(1-benzyl-1, 2, 3-triazoline)-3, 6-endoxohexahydrophthalate

✍ Scribed by N. S. Zefirov; P. P. Kadzyauskas; Yu. K. Yur'ev

Book ID
112490717
Publisher
Springer US
Year
1965
Tongue
English
Weight
172 KB
Volume
1
Category
Article
ISSN
0009-3122

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## Abstract A synthesis of C‐chlorinated analogues of 1,5‐diaza‐2,4‐diphosphorinan‐6‐ones is described. The P‐chlorophosphine 3, a key compound for all reported substitution reactions, reacts in an unusual way with N,N′‐dimethyl‐N,N′‐bis(trimethylsilyl)urea to give the unsymmetrical product 5, the